HRID486369

反应详情

EQUATION

反应方程式

HRID 486369 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 4.9 g of trans-4-[2-[2-(3,4-difluorophenyl)-5-pyridyl]vinyl]cyclohexanecarbonitrile in 120 ml of toluene is hydrogenated with 0.5 g of 10 percent palladium/carbon at room temperature and normal pressure. Filtration and evaporation of the filtrate yields trans-4-[2-[2-(3,4-difluorophenyl)-5-pyridyl]ethyl]cyclohexanecarbonitrile.

WORKUP

后处理

  1. filtrationFiltration and evaporation of the filtrate