HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178511233, compound → HCID 178511234, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178511233 | HCID 178511233 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178511234 | HCID 178511234 | — |
Reaction Steps
A solution of 4.9 g of trans-4-[2-[2-(3,4-difluorophenyl)-5-pyridyl]vinyl]cyclohexanecarbonitrile in 120 ml of toluene is hydrogenated with 0.5 g of 10 percent palladium/carbon at room temperature and normal pressure. Filtration and evaporation of the filtrate yields trans-4-[2-[2-(3,4-difluorophenyl)-5-pyridyl]ethyl]cyclohexanecarbonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292452 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-c097127435f1486cbe694bd975baa097 |
| Source note | uspto-grants-1994_03 |