Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 56-03-1 | HCID 5939 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Ethyl isothiocyanate | HCID 10966 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19095468 | HCID 19095468 | 104.9% |
Reaction Steps
To 15 ml of dry dimethylformamide were dissolved 1.52 g of diguanide and 1.31 g of ethylisothiocyanate, and the solution was heated at 100° C. for 4 hours. After cooling, the solution was added to 60 ml of water to produce white precipitates, which subsequently was dried to obtain 2.7 g of the title compound having the characteristics of:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05292733 |
|---|
| Source dataset | uspto-grants-1994_03 |
|---|
| ORD ID | ord-5c3277c045434c12aaf2fd23019c1c57 |
|---|
| Source note | uspto-grants-1994_03 |
|---|
