HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 19095281, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 19095264 | HCID 19095264 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19095281 | HCID 19095281 | 78% |
Reaction Steps
3,4-Dihydro-1-methyl-6-phenylpyrrolo[1,2-a]pyrazine (0.6 g) was dissolved in 10 ml of ethanol and treated with 0.9 ml of methyl iodide under argon. The solution was boiled overnight, cooled and the separated crystals were filtered off. There was obtained 0.8 g (78%) of 3,4-dihydro-1,2-dimethyl-6-phenylpyrrolo[1,2-a]pyrazinium iodide; m.pt.: 213°-216° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292732 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-786d687a092c4f1cadf2ce95761b51cc |
| Source note | uspto-grants-1994_03 |