HRID486628

反应详情

EQUATION

反应方程式

HRID 486628 的结构方程式

PROCEDURE

实验过程

10.5 g of the compound obtained in Stage A in 300 ml of a 48% hydrobromic acid solution, are refluxed for 20 hours. After evaporation and washing twice with ethanol, the residue is taken up in acetone and the mixture then filtered to give 4-(naphth-1-yl)piperidine hydrobromide.

WORKUP

后处理

  1. customAfter evaporation
  2. washwashing twice with ethanol
  3. filtrationthe mixture then filtered