Trifluoroacetic acid → HCID 86747641, compound

HRID 486705Notes

Reaction equation

HRID 486705 reaction equation
[C:1]1([CH2:7][CH2:8][O:9][C:10]2[CH:17]=[CH:16][C:13]([CH:14]=O)=[CH:12][CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:18][C:19](=[O:24])[CH2:20][C:21](=[O:23])[CH3:22].FC(F)(F)C(O)=O.S(Cl)(Cl)=O>>[C:1]1([CH2:7][CH2:8][O:9][C:10]2[CH:17]=[CH:16][C:13]([CH:14]=[CH:18][C:19](=[O:24])[CH2:20][C:21](=[O:23])[CH3:22])=[CH:12][CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

5

Reactant 4

HCID 6422Trifluoroacetic acidHCID 24386Thionyl ChlorideHCID 31261AcetylacetoneHCID 50620744-(2-phenylethoxy)benzaldehyde

Product 1

HCID 86747641HCID 86747641, compound

Procedure

The procedure described in example 8 was repeated by using 5.9 g of 4-(2-phenylethoxy)benzaldehyde, 3.9 ml of 2,4-pentanedione, 26 ml of trifluoroacetic acid and 2.1 ml of thionyl chloride. Yield 4.7 91 an viscous oil.

Workup

  1. customYield 4.7 91 an viscous oil

Sources & evidence

ORD record
ord-816ef8f94f4e4a5092187b0fa0dd421e
Source dataset
uspto-grants-1994_03
Patent number
US05292771

Reaction notes

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