Homoveratrylamine → 3-((2-(3,4-Dimethoxyphenyl)ethyl)amino)butyronitrile

HRID 486805Notes

Reaction equation

HRID 486805 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][NH2:13])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].[C:14](#[N:18])/[CH:15]=[CH:16]/[CH3:17]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH2:11][CH2:12][NH:13][CH:16]([CH3:17])[CH2:15][C:14]#[N:18])[CH:6]=[CH:7][C:8]=1[O:9][CH3:10]

Participants

3

Reactant 2

HCID 8421HomoveratrylamineHCID 637921Crotononitrile

Product 1

HCID 199265973-((2-(3,4-Dimethoxyphenyl)ethyl)amino)butyronitrile

Conditions

Temperature
100 °C

Procedure

A mixture of 10.0 g of 2-(3,4-dimethoxyphenyl)ethylamine with 14 ml of crotononitrile was stirred at 100° C. for 30 h.

Sources & evidence

ORD record
ord-3f8a0cf7a32a4dd08d2e8e75ad0f91ab
Source dataset
uspto-grants-1994_03
Patent number
US05292770

Reaction notes

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