HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-(chloromethyl)benzene → HCID 14677183, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Reactant | HCID 178435257 | HCID 178435257 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 14677183 | HCID 14677183 | 74% |
Reaction Steps
2-ethyl-2-(1H-imidazol-4-yl)-1-indanone and 4-chlorobenzyl chloride were reacted at 60° C. as described in example 5. The yield was 74%. The hydrochloride was prepared in ethyl acetate, m.p. 150°-154° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292887 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-32261ef04fe047c7905f2407f7aba9c6 |
| Source note | uspto-grants-1994_03 |