Ethanol → HCID 23685597, compound

HRID 486922Notes

Reaction equation

HRID 486922 reaction equation
[OH-].[Na+:2].[CH3:3][C:4]([S:9][CH2:10][CH2:11][C:12]1[CH:20]=[CH:19][C:15]2[O:16][CH2:17][O:18][C:14]=2[CH:13]=1)([CH3:8])[C:5]([OH:7])=[O:6].C(O)C>O>[CH3:8][C:4]([S:9][CH2:10][CH2:11][C:12]1[CH:20]=[CH:19][C:15]2[O:16][CH2:17][O:18][C:14]=2[CH:13]=1)([CH3:3])[C:5]([O-:7])=[O:6].[Na+:2]

Participants

5

Reactant 3

HCID 702EthanolHCID 14798Sodium HydroxideHCID 19001629HCID 19001629, compound

Product 1

HCID 23685597HCID 23685597, compoundYield 92.4%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A solution of 0.90 g of sodium hydroxide in 9.0 ml of water was added to 6 g of 2-methyl-2-[{2-(1,3-benzodioxol-5-yl)ethyl}thio]propionic acid to obtain a solution. 100 ml of ethanol was added to the solution and the solvent was distilled off. The residue was washed with ether. After filtration, the product was dried under reduced pressure to obtain 6 g of the intended compound in the form of a white powder.

Workup

  1. customto obtain a solution
  2. distillationthe solvent was distilled off
  3. washThe residue was washed with ether
  4. filtrationAfter filtration
  5. customthe product was dried under reduced pressure

Sources & evidence

ORD record
ord-18829eef9f8a4f35b487af6198367942
Source dataset
uspto-grants-1994_03
Patent number
US05292901

Reaction notes

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