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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 486922Generated: October 30, 2026

Ethanol → HCID 23685597, compound

https://huagongshe.com/reaction/486922

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 19001629HCID 19001629—
SolventWaterHCID 962—
ProductHCID 23685597HCID 2368559792.4%

Reaction Steps

A solution of 0.90 g of sodium hydroxide in 9.0 ml of water was added to 6 g of 2-methyl-2-[{2-(1,3-benzodioxol-5-yl)ethyl}thio]propionic acid to obtain a solution. 100 ml of ethanol was added to the solution and the solvent was distilled off. The residue was washed with ether. After filtration, the product was dried under reduced pressure to obtain 6 g of the intended compound in the form of a white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05292901
Source datasetuspto-grants-1994_03
ORD IDord-18829eef9f8a4f35b487af6198367942
Source noteuspto-grants-1994_03