HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 145592-12-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3,5-Dichloroaniline | HCID 12281 | — |
| Reactant | Ethyl 2-(chlorocarbonyl)-2-methoxypropionate | HCID 19096847 | — |
| Product | 145592-12-7 | HCID 19096872 | 50% |
Reaction Steps
3,5-Dichloroaniline (3.33 grams, 0.02 mole), ethyl 2-(chlorocarbonyl)-2-methoxypropionate (4.0 grams, 0.02 mole), prepared in Example LXII Part C, and triethylamine (2.08 grams, 0.02 mole) were reacted in a manner similar to the procedure described in Example I to give 4.40 grams (0.01 mole) of ethyl 3-[(3,5-dichlorophenyl)amino]-2-methoxy-2-methyl-3-oxopropanoate having a melting point of 72° C.-75° C. Elemental analysis of the product indicated the following:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292937 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-143ed248f74b43038ab64b7ef1a3d970 |
| Source note | uspto-grants-1994_03 |