Methanesulfonic Acid → HCID 88435121, compound

Participants

Reaction Steps

The procedures of Example 8 were repeated, by substituting 3-amino-benzoic acid with 4-amino-phenyl-acetic acid (3 g: 0.0198 mole) and by using 19 g of CH3SO3H instead of 30 g, 2.2 g of H2O2 at 85% (0.055 mole) instead of 2.9 g, and ethyl acetate (300 moles) instead of THF. 5.2 g of crystalline and substantially pure 4-amino-phenyl-peracetic acid methanesulphonate were obtained. Yield: 98.5%.

Provenance & Evidence