HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19094209, compound → HCID 19094249, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19094209 | HCID 19094209 | — |
| Reactant | HCID 19094238 | HCID 19094238 | — |
| Product | HCID 19094249 | HCID 19094249 | 89.3% |
Reaction Steps
The procedure of Example 1(iii and iv) was followed using 5-chloro-2-[(2-chlorophenyl)methyl]amino-3-nitrobenzoic acid (1.50 g, 4.40 mmol) in place of 5-bromo-2-[(2-chlorophenyl)methyl]amino-3-nitrobenzoic acid to give 1.48 g (89.3%) of the title compound, which was recrystallized from methanol; mp 261°-262° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05294631 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-3febf5f307dd489e8711f9727d5bc448 |
| Source note | uspto-grants-1994_03 |