HuagongsheHuagongshe Chemistry Print Report · For research reference only
Gamma-Butyrolactone → 1-Octadecylpyrrolidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Gamma-Butyrolactone | HCID 7302 | — |
| Reactant | Dodecylamine | HCID 13583 | — |
| Reactant | Octadecylamine | HCID 15793 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-Octadecylpyrrolidin-2-one | HCID 81926 | 96% |
Reaction Steps
The procedure described in Example I was repeated except that octadecylamine (Armeen 18D) was substituted for n-dodecylamine and the product was stripped of water and excess butyrolactone and was discharged at about 75° C. to provide 96% pure N-octadecyl-2-pyrrolidone solid in a yield of 96%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05294644 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-a89195aaace64e34b5b1e4776d878a07 |
| Source note | uspto-grants-1994_03 |