HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 1-(2-Methoxy-2-oxoethyl)pyridinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Methyl chloroacetate | HCID 7295 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 1-(2-Methoxy-2-oxoethyl)pyridinium chloride | HCID 11769267 | — |
Reaction Steps
Pyridine (1 equivalent) and methyl chloroacetate (1 equivalent) in ethyl acetate were heated (80° C.) for 24 hours. The reaction mixture was cooled to room temperature and the resulting crystalline pyridinium salt filtered, washed with ethyl acetate, and dried in vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05294721 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-d6f60419ed23424aa2a11487ac3fbb00 |
| Source note | uspto-grants-1994_03 |