反应详情

Pyridine (1 equivalent) and methyl chloroacetate (1 equivalent) in ethyl acetate were heated (80° C.) for 24 hours. The reaction mixture was cooled to room temperature and the resulting crystalline pyridinium salt filtered, washed with ethyl acetate, and dried in vacuum.

1. filtrationthe resulting crystalline pyridinium salt filtered
2. washwashed with ethyl acetate
3. customdried in vacuum