Ethane, 2-bromo-1,1-diethoxy- → HCID 10777837, compound

HRID 487432Notes

Reaction equation

HRID 487432 reaction equation
[C:1]([O:5][C:6](=[O:10])[C@H:7]([CH3:9])[NH2:8])([CH3:4])([CH3:3])[CH3:2].Br[CH2:12][CH:13]([O:17][CH2:18][CH3:19])[O:14][CH2:15][CH3:16]>>[C:1]([O:5][C:6](=[O:10])[C@H:7]([CH3:9])[NH:8][CH2:12][CH:13]([O:17][CH2:18][CH3:19])[O:14][CH2:15][CH3:16])([CH3:4])([CH3:3])[CH3:2]

Participants

3

Reactant 2

HCID 74852Ethane, 2-bromo-1,1-diethoxy-HCID 89016L-Alanine 1,1-dimethylethyl ester

Product 1

HCID 10777837HCID 10777837, compound

Procedure

L-Alanine-t-butyl ester was allowed to react with 2-bromo-1,1-diethoxyethane in substantially the same manner as in Working Example 52 to afford the title compound as a yellowish brown oily product.

Sources & evidence

ORD record
ord-c11e258aa67043b68be38b90aa1fab36
Source dataset
uspto-grants-1994_03
Patent number
US05294713

Reaction notes

Loading…