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HRID487516

反应详情

EQUATION

反应方程式

HRID 487516 的结构方程式

REACTANTS

反应物

3
结构：CCCC(C)Br
HCID7890

Pentane, 2-bromo-

C5H11Br

结构：BrP(Br)Br
HCID24614

Phosphorus tribromide

Br3P

结构：CCCC(C)CC(C)O
HCID143345

2-Heptanol, 4-methyl-

C8H18O

PRODUCTS

生成物

1
结构：CCCC(C)CC(C)Br
HCID15332453

2-Bromo-4-methylheptane

C8H17Br

PROCEDURE

实验过程

17.50 g (0.135 mol) of 4-methylheptan-2-ol (3) was treated with PBr3 (13.48 g, 0.050 mol) as described above in the manufacture of 2-bromopentane (2). The product was purified by distillation at 165°-185° C. to yield 2-bromo-4methylheptane (4).

WORKUP

后处理

  1. distillationThe product was purified by distillation at 165°-185° C.