HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 19092180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 5-(4'-(Bromomethyl)(1,1'-biphenyl)-2-yl)-1-trityl-1H-tetraazole | HCID 10053461 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19092180 | HCID 19092180 | 94.5% |
Reaction Steps
A mixture of 4.0 g of 5-[4'-(bromomethyl)[1,1'-biphenyl]-2-yl]-1-(triphenylmethyl)-1H-tetrazole and 2.2 g of potassium iodide in 50 ml of acetone is heated at reflux for 50 minutes. The reaction mixture is filtered and the filtrate evaporated in vacuo to a residue which is stirred with cold water and the resulting solid collected by filtration, washed with water and air dried to give 4.1 g of the desired product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05296480 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-5f76242733484dd2be7057bf235c2cf2 |
| Source note | uspto-grants-1994_03 |