Water → HCID 19092277, compound

HRID 487575Notes

Reaction equation

[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH2:15][CH2:14][C:13](=O)[CH2:12][CH2:11]2)=[CH:6][CH:5]=1)([O-:3])=[O:2].[C:17]1([CH:23]2[CH2:28][CH2:27][NH:26][CH2:25][CH2:24]2)[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1.O>>[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH2:15][CH2:14][CH:13]([N:26]3[CH2:27][CH2:28][CH:23]([C:17]4[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=4)[CH2:24][CH2:25]3)[CH2:12][CH2:11]2)=[CH:6][CH:5]=1)([O-:3])=[O:2]

Participants

Reactant 3

HCID 962Water

HCID 698734-Phenylpiperidine

HCID 38425621-(4-Nitrophenyl)piperidin-4-one

Product 1

HCID 19092277HCID 19092277, compound

Procedure

3.0 g of 1-(4-nitrophenyl) -4-piperidone and 2.2 g of 4-phenylpiperidine were reacted as in Example 1. The product contained 1/6 mol of water of crystallization.

Sources & evidence

ORD record: ord-f0464dcf8d554499ae6d94d28b87bf00
Source dataset: uspto-grants-1994_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05296485

Reaction notes

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