HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19092277, compound → HCID 19092270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19092277 | HCID 19092277 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19092270 | HCID 19092270 | — |
Reaction Steps
0.5 g of palladium carbon (containing 10% by weight palladium) was added to a solution of 1.2 g (2.7 mmol) of 1-(4-nitrophenyl)-4-(4-phenyl-1-piperidinyl)piperidine (cf. Example 8) in 100 ml of methanol. Hydrogenation was continued until hydrogen uptake ceased, then the solids were filtered off and the solvent was removed under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05296485 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-3fbb6811595a4c1a8c8a1164181806be |
| Source note | uspto-grants-1994_03 |