HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19092245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(Trifluoromethyl)benzylamine | HCID 75962 | — |
| Reactant | 4-Chloroquinazoline | HCID 78864 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19092245 | HCID 19092245 | — |
Reaction Steps
A mixture of 1.65 g of 4-chloroquinazoline, 1.5 g of [3-(trifluoromethyl)phenyl]methyl amine, and 1.0 g of triethylamine in 50 ml of ethanol was refluxed for 6 hours. The mixture was then cooled, and washed with water. After removing solvents in vacuo the product was crystallized from a mixture of ethyl acetate and hexane. Yield: 1.0 g. M.P. 145°-146° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05296484 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-0ef60508583a45ad94a2cc4c9cf15cfe |
| Source note | uspto-grants-1994_03 |