Hydrochloric Acid → HCID 131718353, compound

Participants

Reaction Conditions

Reaction Steps

A solution of chloracetimidoethylether, hydrochloride (1.58 g, 10 mmol) and N-methyl-ethylenediamine (0.74 g, 10 mmol) in 10 ml absolute ethanol is stirred at 0° C. and under a nitrogen atmosphere for one hour. A solution of hydrogen chloride in absolute ethanol (6.3 ml, 10 mmol) is added and the mixture is heated to 40° C. and stirred for additional two hour. After cooling to room temperature a precipitate of ammonium chloride is filtered of and the filtrate is concentrated in vacuo yielding the title compound as a yellow oil.

Provenance & Evidence