Hydrochloric Acid → HCID 131718353, compound

HRID 487582Notes

Reaction equation

HRID 487582 reaction equation
[ClH:1].[CH3:2][NH:3][CH2:4][CH2:5][NH2:6].[Cl-].[NH4+].[CH2:9](O)[CH3:10]>>[ClH:1].[CH3:2][N:3]1[CH2:4][CH2:5][N:6]=[C:10]1[CH2:9][Cl:1]

Participants

5

Reactant 4

HCID 313Hydrochloric Acid2×HCID 702Ethanol2×HCID 8014N-MethylethylenediamineHCID 25517Ammonium Chloride

Product 1

HCID 131718353HCID 131718353, compound

Conditions

Temperature
40 °C

Procedure

A solution of chloracetimidoethylether, hydrochloride (1.58 g, 10 mmol) and N-methyl-ethylenediamine (0.74 g, 10 mmol) in 10 ml absolute ethanol is stirred at 0° C. and under a nitrogen atmosphere for one hour. A solution of hydrogen chloride in absolute ethanol (6.3 ml, 10 mmol) is added and the mixture is heated to 40° C. and stirred for additional two hour. After cooling to room temperature a precipitate of ammonium chloride is filtered of and the filtrate is concentrated in vacuo yielding the title compound as a yellow oil.

Workup

  1. filtrationis filtered of and the filtrate
  2. concentrationis concentrated in vacuo

Sources & evidence

ORD record
ord-b4125f3dffe4477791f7e996ee596eae
Source dataset
uspto-grants-1994_03
Patent number
US05296493

Reaction notes

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