HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) → HCID 18961046, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) | HCID 78397 | — |
| Reactant | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| Reactant | HCID 11333231 | HCID 11333231 | — |
| Product | HCID 18961046 | HCID 18961046 | 7.5% |
Reaction Steps
Following a procedure similar to that described in Example 1, but using 112 mg of 2-oxo-4-phenyloxazolidine-5-carboxylic acid, 110 mg of N-(2-nitrooxyethyl)amine nitrate and 0.24 ml of diphenylphosphoryl azide, 12 mg of the title compound were obtained as colorless crystals, melting at 122°-124° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298516 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-1828d407960f490a8d7f28db67f24b7c |
| Source note | uspto-grants-1994_03 |