HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dodecanoyl chloride → HCID 19019876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dodecanoyl chloride | HCID 8166 | — |
| Reactant | 3-Furancarboxaldehyde, 5-(triethylsilyl)- | HCID 10878438 | — |
| Reactant | HCID 15037119 | HCID 15037119 | — |
| Reactant | HCID 54351447 | HCID 54351447 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 19019876 | HCID 19019876 | — |
Reaction Steps
4-(1,2-Dihydroxyethyl)-2-triethylsilylfuran (prepared substantially as described above using 5-triethylsilyl-3-furaldehyde in place of the corresponding trimethylsilyl furaldehyde) is reacted with dodecanoyl chloride in the presence of triethylamine to give 4-(1-hydroxy-2-dodecanoyloxyethyl)-2-triethylsilylfuran. Treating this 1-hydroxy compound with acetic anhydride and pyridine gives 4-(1-acetoxy-2-dodecanoyl-oxyethyl)-2-triethylsilylfuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298633 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-9b7dec9a1b4e4492bca6710952534c2d |
| Source note | uspto-grants-1994_03 |