Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → HCID 19091770, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Diethyl iminodiacetate | HCID 80502 | — |
| 반응물 | 3,5-Bis[(11-methoxy-11-oxoundecyl)oxy]benzoic acid | HCID 19091815 | — |
| 생성물 | HCID 19091770 | HCID 19091770 | — |
반응 단계
Conversion of 3,5-bis[(11-methoxy-11-oxoundecyl)oxy]benzoic acid to the acid chloride with thionyl chloride followed by treatment with diethyl iminodiacetate as in Example 21 gave N-(2-ethoxy-2-oxoethyl)-N-[3,5-bis[(11-methoxy-11-oxoundecyl)oxy]-benzoyl]glycine ethyl ester as an oil after chromatography on 125 g of silica gel using 20% ethyl acetate-hexane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05298652 |
| 출처 데이터셋 | uspto-grants-1994_03 |
| ORD ID | ord-4bce587ed8fb44b799c628fdff238b49 |
| 출처 메모 | uspto-grants-1994_03 |