HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl iminodiacetate → N-(2-ethoxy-2-oxoethyl)-N-[5-(decyloxy)-2-(phenylmethoxy)benzoyl]glycine ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl iminodiacetate | HCID 80502 | — |
| Reactant | 5-(Decyloxy)-2-(phenylmethoxy)benzoic acid chloride | HCID 54166966 | — |
| Product | N-(2-ethoxy-2-oxoethyl)-N-[5-(decyloxy)-2-(phenylmethoxy)benzoyl]glycine ethyl ester | HCID 19091876 | 82% |
Reaction Steps
The reaction of 5-(decyloxy)-2-(phenylmethoxy)benzoic acid chloride with diethyl iminodiacetate under conditions described in Example 80 gave N-(2-ethoxy-2-oxoethyl)-N-[5-(decyloxy)-2-(phenylmethoxy)benzoyl]glycine ethyl ester (82% yield, mp 37°-38°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298652 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-5b56015db2c4441386c93dbf195ce385 |
| Source note | uspto-grants-1994_03 |