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Sodium Hydroxide → 5-[[6-([1,1'-Biphenyl]-4-yloxy)hexyl]oxy]-2-(phenylmethoxy)benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | HCID 54022805 | HCID 54022805 | — |
| 生成物 | 5-[[6-([1,1'-Biphenyl]-4-yloxy)hexyl]oxy]-2-(phenylmethoxy)benzoic acid | HCID 19091869 | 96% |
反応手順
Sodium hydroxide hydrolysis of 5-[[6-([1,1'-biphenyl]-4-yloxy)hexyl]oxy]-2-(phenylmethoxy)benzoic acid methyl ester as described in Example 60 gave 5-[[6-([1,1'-biphenyl]-4-yloxy)hexyl]oxy]-2-(phenylmethoxy)benzoic acid (96% yield, mp 131°-133°).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05298652 |
| 出典データセット | uspto-grants-1994_03 |
| ORD ID | ord-78eaf07b5b034d7c9736d93ff02701db |
| 出典メモ | uspto-grants-1994_03 |