HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Gentisate → 2-Hydroxy-5-[(12-phenoxydodecyl)oxy]benzoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Gentisate | HCID 75077 | — |
| Reactant | 12-Phenoxydodecyl bromide | HCID 12369904 | — |
| Product | 2-Hydroxy-5-[(12-phenoxydodecyl)oxy]benzoic acid methyl ester | HCID 54337001 | 75% |
Reaction Steps
The reaction of 2,5-dihydroxybenzoic acid methyl ester with 12-phenoxydodecyl bromide under condition described in Example 101 gave 2-hydroxy-5-[(12-phenoxydodecyl)oxy]benzoic acid methyl ester (75% yield, mp 61°-64° ).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298652 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-582dfdeab3954227ad404ba348fbf280 |
| Source note | uspto-grants-1994_03 |