HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 5-[(12-Phenoxydodecyl)oxy]-2-(phenylmethoxy)benzoic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 2-Hydroxy-5-[(12-phenoxydodecyl)oxy]benzoic acid methyl ester | HCID 54337001 | — |
| Product | 5-[(12-Phenoxydodecyl)oxy]-2-(phenylmethoxy)benzoic acid methyl ester | HCID 53929860 | 58% |
Reaction Steps
The reaction of 2-hydroxy-5-[(12-phenoxydodecyl)oxy]benzoic acid methyl ester with benzyl bromide as described in Example 102 gave 5-[(12-phenoxydodecyl)oxy]-2-(phenylmethoxy) benzoic acid methyl ester (58% yield, mp 46°-48° ).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05298652 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-d838399133d7425e9f06595ba3614af6 |
| Source note | uspto-grants-1994_03 |