HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Nitrophenyl)acetic acid → HCID 53833682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Nitrophenyl)acetic acid | HCID 4661 | — |
| Reactant | Veratraldehyde | HCID 8419 | — |
| Solvent | Piperidine | HCID 8082 | — |
| Product | HCID 53833682 | HCID 53833682 | 34% |
Reaction Steps
The title compound was prepared from p-nitrophenylacetic acid (25.0 g, 0.14 mol), and 3,4-dimethoxybenzaldehyde (21.0 g, 0.14 mol) in piperidine (5 mL) using the procedure described in Example 1, Step A, to yield a yellow solid, 13.4 g (0.047 mol, 34%) of the desired product. mp: 133-134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06972287B1 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-fea97c4fa99240cbb5bca671e97e63ef |
| Source note | uspto-grants-2005_12 |