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HRID488494

反应详情

EQUATION

反应方程式

HRID 488494 的结构方程式

REACTANTS

反应物

1
结构：COc1cc(C=Cc2ccc([N+](=O)[O-])cc2)cc(OC)c1OC
HCID54348404

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(CCc2ccc(N)cc2)cc(OC)c1OC
HCID364705

4-[2-(3,4,5-trimethoxyphenyl)ethyl]aniline

C17H21NO3

收率 76.7%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Ni]
催化剂HCID935

Nickel

Ni

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

The title compound was prepared from 1,2,3-trimethoxy-5-[2-(4-nitrophenyl)ethenyl]benzene (9.5 g, 0.03 mol) and Ra—Ni (1.0 g) in THF (50 mL) at 21-26° C. (ΔP=9.6 psi) under a hydrogen atmosphere using the procedure described in Example 1, Step B. This procedure yielded a tan powder, 6.6 g (0.023 mol, 74%) of the desired product. mp 91-93° C.