Boron tribromide → HCID 22269771, compound

Participants

Reaction Steps

The title compound was prepared from 2-{4-[2-(3,4,5-trimethoxy-phenyl)-ethyl]phenylamino}benzoic acid (0.50 g, 1.23 mmol) in CH2Cl2 (40 mL) and BBr3 (10 mL, 1M in CH2Cl2, 10.0 mmol) using the procedure described in Example 4, Step D. This procedure yielded a green solid, 0.25 g (0.68 mmol, 65%) of the desired product. mp: 160.0-162.0° C.

Provenance & Evidence