2-Bromobenzoic acid → Potassium o-bromobenzoate

HRID 488519Notes

Reaction equation

HRID 488519 reaction equation
[Br:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].C([O-])([O-])=O.[K+:15].[K+]>CO>[K+:15].[Br:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([O-:6])=[O:5]

Participants

4

Reactant 2

HCID 69402-Bromobenzoic acidHCID 11430Potassium Carbonate

Product 1

HCID 19205467Potassium o-bromobenzoateYield 100%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a solution of o-bromobenzoic acid (201.03 g, 1.0 mol) in MeOH (500 mL), K2CO3 (69 g, 1.0 mol) was added. The mixture was concentrated to give the desired product (239.1 g, 1.0 mol, 100%).

Workup

  1. concentrationThe mixture was concentrated

Sources & evidence

ORD record
ord-b4a99f89d297472d85cdefa58996d216
Source dataset
uspto-grants-2005_12
Patent number
US06972287B1

Reaction notes

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