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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 488998Generated: October 29, 2026

Trifluoroacetic acid → HCID 23387352, compound

https://huagongshe.com/reaction/488998

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 23387543HCID 23387543—
SolventDichloromethaneHCID 6344—
ProductHCID 23387352HCID 23387352—

Reaction Steps

To a solution of 4-methoxybenzyl 2-(N-CBZ-L-valyloxy)-propionate (7.8 g, 17.5 mmole) in dichloromethane (100 ml) was added trifluoroacetic acid (10 ml) and the solution was stirred for one hour at room temperature. The solution was evaporated under reduced pressure and the product was isolated by silica gel column chromatography. Yield: 5.0 g

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06974802B2
Source datasetuspto-grants-2005_12
ORD IDord-90922862826941529dbf6fb52685a912
Source noteuspto-grants-2005_12