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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 489004Generated: October 30, 2026

HCID 57433140, compound → HCID 23387539, compound

https://huagongshe.com/reaction/489004

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 57433140HCID 57433140—
CatalystPalladiumHCID 23938—
SolventEthylacetate methanolHCID 21584119—
ProductHCID 23387539HCID 23387539—

Reaction Steps

To a solution of 4-(N-Boc-L-valyloxy)butyric acid benzyl ester (1.2 g, 3 mmole) in ethyl acetate/methanol (5 ml/5 ml) was added palladium black (20 mg). The reaction mixture was kept under hydrogen at atmospheric pressure for 2 hr. The suspension was filtered through Celite and dried, giving the title product, 840 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06974802B2
Source datasetuspto-grants-2005_12
ORD IDord-4a63b585d06f4c5497bf74118ad1d5f3
Source noteuspto-grants-2005_12