Hydrochloric Acid → HCID 69140350, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in Step (e) using N-[(1R)-1-[(4-chlorophenyl)methyl]-2-(4-{2-[(methylsulfonyl)-amino]phenyl}piperidyl)-2-oxoethyl](tert-butoxy)-carboxamide (Step f) (250 mg, 0.50 mmol) and a saturated soln of HCl in EtOAc (10 mL). The title compound (HCl salt) was isolated by filtration as a white solid (195 mg, 83%). MS (ESI, pos. ion) m/z: 473 (M+1). Calc'd for C21H27Cl2N3O3S: 472.43.

Provenance & Evidence