Hydrochloric Acid → HCID 69141554, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in Example 1 (Step e) using N-((1R)-1-[(4-chlorophenyl)methyl]-2-(4-[2-(hydroxyethyl)phenyl]piperidyl)-2-oxoethyl)(tert-butoxy)carboxamide (Step d) (0.976 g, 2.0 mmol) and satd anhydrous HCl in EtOAc (30 mL). The title compound was obtained as a white solid (0.846 g). MS (ESI, pos. ion) m/z: 387 (M+1) MS (EST, neg. ion) m/z: 385 (M−1). Calc'd for C22H27ClN2O2: 386.18.

Provenance & Evidence