Hydrochloric Acid → HCID 23587439, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in Example 16 (Step b) from N-[(1R)-1-[(4-chlorophenyl)methyl]-2-(4-{2-[(fluoren-9-ylmethoxy)carbonylamino]-phenyl}piperidyl)-2-oxoethyl](tert-butoxy)carboxamide (Step c) (6.8 g, 10 mmol) and satd anhydrous HCl in EtOAc (50 mL). The title compound was obtained as a white solid (6.1 g). MS (ESI, pos. ion) m/z: 580 (M+1); MS (ESI, neg. ion) m/z: 578 (M−1). Calc'd for C35H35Cl2N3O3: 579.23.

Provenance & Evidence