HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl 4-oxopiperidine-1-carboxylate → HCID 69694350, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Reactant | HCID 7183045 | HCID 7183045 | — |
| Product | HCID 69694350 | HCID 69694350 | 69% |
Reaction Steps
(3R)-Morpholin-4-yl-piperidin-3-yl-methanone (2.25 g, 11.4 mmol) was reacted with tert-butyl 4-oxo-1-piperidinecarboxylate (1 eq., 2.27 g) under conditions analogous to those described above for the preparation of Intermediate 1 to give (3R)-3-(morpholine-4-carbonyl)-[1,4′]bipiperidinyl-1′-carboxylic acid tert-butyl ester (3.00 g, 69%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06979741B2 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-360533240eb74414a6f66da6a9ec2bbe |
| Source note | uspto-grants-2005_12 |