HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178505591, compound → HCID 178505595, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178505591 | HCID 178505591 | — |
| Solvent | Benzylamine | HCID 7504 | — |
| Product | HCID 178505595 | HCID 178505595 | 95% |
Reaction Steps
This compound was synthesize by refluxing 2-chloro-4-[3-(4-fluorophenyl)-1H-pyrazol-4-yl]pyrimidine prepared in accordance with Example A-299 in benzylamine overnight. The product, 4-[3-(4-fluorophenyl)-1H-pyrazol-4-yl]-N-(phenylmethyl)-2-pyrimidinamine, was obtained as a white solid in 95% yield; mp: 216-217° C.; Anal. Calc'd for C20H16FN5: C, 69.55; H, 4.67; N, 20.28. Found: C, 69.73; H, 4.69; N, 19.90.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06979686B1 |
| Source dataset | uspto-grants-2005_12 |
| ORD ID | ord-e8610580900343a4ad4946dd26329e3b |
| Source note | uspto-grants-2005_12 |