HCID 131727436, compound → HCID 57217836, compound

Participants

Reaction Steps

1.25 g of the compound obtained in step 5-3 and 250 mg of 10% palladium-carbon were stirred for 1 hour at room temperature and under a hydrogen atmosphere in 12.5 mL of methanol. The insolubles were filtered off and the filtrate was concentrated under reduced pressure to obtain 704 mg of the titled compound (colorless oily substance).

Provenance & Evidence