HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67428575, compound → HCID 45115932, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67428575 | HCID 67428575 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 45115932 | HCID 45115932 | 109.2% |
Reaction Steps
A suspension of 1.80 g of the compound obtained in step 8-1 and 360 mg of 10% palladium-carbon in 36 mL of methanol was stirred for 3 hours at room temperature and under hydrogen atmosphere. The insolubles were filtered off and the reaction mixture was concentrated under reduced pressure to obtain 1.07 g of the titled compound. This compound was used in the following reaction without being purified.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07528124B2 |
| Source dataset | uspto-grants-2009_05 |
| ORD ID | ord-9160562361dc4d18aac252bfaf5a6439 |
| Source note | uspto-grants-2009_05 |