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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 490138Generated: October 31, 2026

HCID 67428575, compound → HCID 45115932, compound

https://huagongshe.com/reaction/490138

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67428575HCID 67428575—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 45115932HCID 45115932109.2%

Reaction Steps

A suspension of 1.80 g of the compound obtained in step 8-1 and 360 mg of 10% palladium-carbon in 36 mL of methanol was stirred for 3 hours at room temperature and under hydrogen atmosphere. The insolubles were filtered off and the reaction mixture was concentrated under reduced pressure to obtain 1.07 g of the titled compound. This compound was used in the following reaction without being purified.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07528124B2
Source datasetuspto-grants-2009_05
ORD IDord-9160562361dc4d18aac252bfaf5a6439
Source noteuspto-grants-2009_05