反应详情

A solution of D6 (10 g, 3.4 mmol) in methanol (150 ml) was hydrogenated at 50 psi in a Parr hydrogenator using 10% Palladium on carbon catalyst (800 mg) for 18 h. Catalyst was filtered off and the filtrate concentrated under reduced pressure to afford the product as a white solid.

1. customfor 18 h
2. filtrationCatalyst was filtered off
3. concentrationthe filtrate concentrated under reduced pressure