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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 490911Generated: October 30, 2026

Hydrochloric Acid → HCID 67529443, compound

https://huagongshe.com/reaction/490911

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 57675199HCID 57675199—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 67529443HCID 67529443—

Reaction Conditions

Temperature20 °C

Reaction Steps

A solution of hydrogen chloride in dioxane (1 ml) was added to Intermediate 124 (0.052 g, 0.1 mmol) and the reaction mixture stirred at 20° C. for 2 hours. The solution was evaporated in vacuo to afford Intermediate 125 as a yellow solid (0.047 g). LCMS showed MH+=412; TRET=2.21 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07528148B2
Source datasetuspto-grants-2009_05
ORD IDord-b695aa737e9442999043927f61e55009
Source noteuspto-grants-2009_05