huagongshe.com
HRID490960

反应详情

EQUATION

反应方程式

HRID 490960 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2[nH]c(SCc3ncc(C)c(OC)c3C)nc2n1
HCID9840489

5-Methoxy-2-{[(4-methoxy-3,5-dimethylpyridin-2-yl)methyl]sulfanyl}-1H-imidazo[4,5-b]pyridine

C16H18N4O2S

结构：CC(C)c1ccccc1.[O-]O
HCID53627471

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2[nH]c([S@@](=O)Cc3ncc(C)c(OC)c3C)nc2n1
HCID11552393

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

CONDITIONS

反应条件

温度
20 °C

PROCEDURE

实验过程

A solution in DMF (6 volumes) of 5-methoxy-2-[[(4-methoxy-3,5-dimethyl-2-pyridinyl)-methyl]thio]imidazo[4,5-b]pyridine (100 mg, 0.303 mmol) is added under stirring at 20° C., immediately followed by cumene hydroperoxide (80%, 65 μL, 0.352 mmol)