HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 69436130, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | N-methyl-2-oxoindoline-5-sulfonamide | HCID 10176909 | — |
| Reactant | 4-methoxy-1H-indole-2-carbaldehyde | HCID 10678838 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69436130 | HCID 69436130 | — |
Reaction Steps
A mixture of 2-oxo-2,3-dihydro-1H-indole-5-sulfonic acid methylamide (194 mg, 0.86 mmol), 4-methoxy-1H-indole-2-carbaldehyde (150 mg, 0.86 mmol) and piperidine (36 mg, 0.43 mmol) in ethanol (0.2M) was stirred at room temperature for a total of 5 days. The reaction was concentrated to ¼ of its volume and the precipitate was collected by vacuum filtration to give the title compound as a pale orangish-red solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06706709B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-04e993e7259643b294fbed62d7615853 |
| Source note | uspto-grants-2004_03 |