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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 491251Generated: October 27, 2026

Azobisisobutyronitrile → Bromostyrene acrolein methacrylate

https://huagongshe.com/reaction/491251

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAzobisisobutyronitrileHCID 6547—
ReactantAcroleinHCID 7847—
ReactantPropylene glycol methyl ether acetateHCID 7946—
Reactant4-BromostyreneHCID 16263—
ReactantMethacrylateHCID 87595—
ProductBromostyrene acrolein methacrylateHCID 86612195—

Reaction Conditions

Temperature67 °C

Reaction Steps

3 g of 4-bromostyrene, 4 g of acrolein, 3 g of methacrylate and 0.2 g of AIBN were sufficiently mixed with 50 g of PGMEA. The mixture was polymerized by heating the mixture at 67° C. for 8 hours. After completion of the polymerization, the polymerization product was precipitated in n-hexane, filtered, and dried in vacuo to give a poly(bromostyrene-acrolein-methacrylate) copolymer.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07531297B2
Source datasetuspto-grants-2009_05
ORD IDord-56c73c674f6e45feb107ca90d3d30919
Source noteuspto-grants-2009_05