Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 10907393, 화합물 → Fmoc-Ser-OTce
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 10907393 | HCID 10907393 | — |
| 용매 | Trifluoroacetic acid water | HCID 22392675 | — |
| 생성물 | Fmoc-Ser-OTce | HCID 10939458 | — |
반응 단계
Fmoc-Ser(tBu)-OTce was dissolved in TFA-H2O (19:1, 10 mL) and allowed to stir for 5 h. The reaction mixture was concentrated in vacuo and purified by flash chromatography (EtOAc-Hexane, 3:7) to give Fmoc-Ser-OTce (0.83 g, 1.8 mmol, 69% overall yield for the two steps).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07531506B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-cc852d7cc92a428a8e27c521f023d20a |
| 출처 메모 | uspto-grants-2009_05 |